Static Headspace-Gas Chromatography Theory and Practice - gebrauchtes Buch

EAN (ISBN-13): 9780471749448
ISBN (ISBN-10): 0471749443
Gebundene Ausgabe
Erscheinungsjahr: 2006
Herausgeber: Wiley-Interscience
349 Seiten
Gewicht: 0,635 kg
Sprache: eng/Englisch

Buch in der Datenbank seit 2007-05-29T12:02:35+02:00 (Berlin)
Detailseite zuletzt geändert am 2023-11-30T11:33:37+01:00 (Berlin)
ISBN/EAN: 9780471749448

ISBN - alternative Schreibweisen:
0-471-74944-3, 978-0-471-74944-8
Alternative Schreibweisen und verwandte Suchbegriffe:
Autor des Buches: kolb, bruno, ettre, leslie
Titel des Buches: rom, static, chromatography, sorry out gas, headspace, theory wants, the practice

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Daten vom Verlag:

Autor/in: Bruno Kolb; Leslie S. Ettre
Titel: Static Headspace-Gas Chromatography - Theory and Practice
Verlag: Wiley-Interscience; John Wiley & Sons
376 Seiten
Erscheinungsjahr: 2006-06-13
Gewicht: 0,630 kg
Sprache: Englisch
162,00 € (DE)
Not available (reason unspecified)
160mm x 238mm x 22mm

BB; Hardcover, Softcover / Chemie; Chromatographie; Chemie; Chemistry; Chromatographie / Trennverfahren; Chromatography / Separation Techniques; Gaschromatographie; Chromatographie / Trennverfahren

Preface. Preface to the First Edition. List of Acronyms and Symbols. 1. General introduction. 1.1 Principles of headspace analysis . 1.2 Types of headspace analysis. 1.3 The evolution of the HS-GC methods. 1.4 Headspace -- gas chromatography literature. 1.5 Regulatory methods utilizing (static) HS-GC. 1.6 References. 2. Theoretical background of HS-GC and its applications. 2.1 Basic theory of headspace analysis. 2.2 Basic physicochemical relationships. 2.3 Headspace sensitivity. 2.4 Headspace linearity. 2.5 Duplicate analyses. 2.6 Multiple headspace extraction (MHE). 2.7 References. 3. The technique of HS-GC. 3.1 Sample vials. 3.2 Caps. 3.3 Septa. 3.4 Thermostatting. 3.5 The fundamentals of headspace sampling systems. 3.6 Use of open-tubular (capillary) columns. 3.7 Enrichment techniques in HS-GC. 3.8 Special techniques with the balanced-pressure systems. 3.9. Reaction HS-GC. 3.10 References. 4. Sample handling in HS-GC. 4.1 Equilibration. 4.2 Solution approach. 4.3 Sample handling and sample introduction. 4.4 Preparation of standard solutions. 4.5 Influence of the matrix. 4.6 Methods aiming the complete evaporation of the analyte. 4.7 References. 5. Headspace methods for quantitative analysis. 5.1 Internal normalization. 5.2 Internal standard method. 5.3 External standard method. 5.4 Standard addition method. 5.5 Multiple headspace extraction (MHE). 5.6 Analysis of solid samples (adsorption systems). 5.7 Calibration techniques with headspace samples of varying volumes. 5.8 Analysis of gas samples. 5.9 References. 6. Method development in HS-GC. 6.1 General guidelines. 6.2 Determination of the residual monomer content of polystyrene pellets. 6.3 Determination of residual solvents in a printed plastic film. 6.4 Determination of the volatile constituents of a cathodic electrolytic plating bath. 7. Nonequilibrium static headspace analysis. 7.1 Accelerated analysis. 7.2 Heat-sensitive samples. 7.3 References. 8. Qualitative analysis by HS-GC. 8.1 The use of HS-GC in 'fingerprinting.'. 8.2 The use of headspace sampling in hyphenated systems. 8.3 The use of HS-GC in microbiology. 8.4 References. 9. Special measurements. 9.1 Determination of vapor pressures. 9.2 Determination of activity coefficients. 9.3 Determination of related physicochemical functions. 9.4 Determination of phase distribution (partition coefficient). 9.5 Reaction constant measurements. 9.6 Determination of solute solubility by MHE. 9.7 Gas-solid systems. 9.8 Validation of the headspace instrumentation: investigation of detector linearity and detection limit. 9.9 References. Index.